Page 77 - 《中国药房》2021年16期
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400                              15 000
                                                                            5 000
          300                              10 000
          intensity  200                  intensity                         intensity  2 500

          100                              5 000
           0                                  0                               0
            0      2.5    5.0    7.5           0     2.5   5.0    7.5   10.0   0     2.5    5.0   7.5   10.0
                       t,min                               t,min                            t,min
         1 500                                                              50 000
                                           40 000

         1 000                             30 000
         intensity                        intensity  20 000                intensity  25 000
          500
                                           10 000

           0                                  0                               0
             0     2.5     5.0    7.5          0     2.5   5.0    7.5   10.0   0     2.5    5.0   7.5   10.0
                       t,min                               t,min                            t,min

                                           5 000                            7 500
         1 000
         intensity  500                    intensity  2 500                 intensity  5 000
                                                                            2 500

           0                                 0                                0
             0     2.5     5.0    7.5          0     2.5   5.0    7.5   10.0   0     2.5    5.0   7.5    10.0
                       t,min                               t,min                            t,min
          200
                                           15 000
          150                                                                500
          intensity  100                  intensity  10 000                  intensity  250

           50                               5 000
            0                                 0                               0
             0      2.5    5.0    7.5          0     2.5   5.0    7.5   10.0    0     2.5   5.0    7.5   10.0
                       t,min                               t,min                            t,min
          150                                                               4 000
                                           15 000
                                                                            3 000
          100                              10 000
          intensity                       intensity                         intensity  2 000
           50                               5 000
                                                                            1 000
            0                                 0                                0
             0     2.5     5.0    7.5          0     2.5   5.0    7.5   10.0    0     2.5   5.0    7.5   10.0
                       t,min                               t,min                            t,min
          100                              10 000                           4 000
           75                              7 500                            3 000
          intensity  50                   intensity  5 000                  intensity  2 000

           25                              2 500                            1 000
           0                                  0                               0
             0     2.5     5.0    7.5          0     2.5   5.0    7.5   10.0   0     2.5    5.0   7.5    10.0
                       t,min                               t,min                            t,min
                     A. 空白溶液                           B.混合对照品溶液                         C.供试品溶液
           注:1.苯甲酰乌头原碱;2.苯甲酰新乌头原碱;3.苯甲酰次乌头原碱;4.乌头碱;5.新乌头碱;6.次乌头碱;7.胡椒碱;8.没食子酸
           Note:1. benzoylaconitine;2. benzoylneoaconitine;3. benzoylhypoaconitine;4. aconitine;5. neoaconitine;6. hypoaconitine;7. piperine;8. gal-
        lic acid
                                 图 2 苯甲酰乌头原碱等8 种成分的多反应监测模式图谱
                   Fig 2  Multiple reaction monitoring chromatograms of 8 components as benzoylaconitine


        中国药房    2021年第32卷第16期                                            China Pharmacy 2021 Vol. 32 No. 16  ·1991 ·
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