Page 52 - 《中国药房》2022年3期
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5:鞣花酸301.000 0>284.100 0(-)CE:29.0 5:鞣花酸301.000 0>284.100 0(-)CE:29.0 5:鞣花酸301.000 0>284.100 0(-)CE:29.0
700
1 250 000
75 000 600 C5
A5 B5
1 000 000 500
50 000 75 000 mAU 400
mAU mAU 50 000 300
25 000 200
25 000 100
0 0 0
0 2.5 5.0 7.5 0 2.5 5.0 7.5 0 2.5 5.0 7.5
t/min t/min t/min
6:柯里拉京632.900 0>300.900 0(-)CE:41.0 6:柯里拉京632.900 0>300.900 0(-)CE:41.0 6:柯里拉京632.900 0>300.900 0(-)CE:41.0
150 000 3 500 000 75
125 000 3 000 000 C6
A6 B6
100 000 2 500 000 50
mAU 75 000 mAU 2 000 000 mAU
1 500 000
50 000 1 000 000 25
25 000 500 000
0 0 0
0 2.5 5.0 7.5 0 2.5 5.0 7.5 0 1 2 3 4 5 6 7 8 9
t/min t/min t/min
7:莽草酸173.100 0>111.000 0(-)CE:11.0 7:莽草酸173.100 0>111.000 0(-)CE:11.0 7:莽草酸173.100 0>111.000 0(-)CE:11.0
17 500 200 000 1 250
15 000 C7
12 500 A7 150 000 B7 1 000
mAU 10 000 mAU 100 000 mAU 750
7 500
5 000 50 000 500
2 500 250
0 0 0
0 2.5 5.0 7.5 0 2.5 5.0 7.5 0 2.5 5.0 7.5
t/min t/min t/min
8:阿魏酸192.900 0>134.000 0(-)CE:16.0 8:阿魏酸192.900 0>134.000 0(-)CE:16.0 8:阿魏酸192.900 0>134.000 0(-)CE:16.0
3 500 1 250
3 000 1 000 75 C8
2 500 A8 750 B8
mAU 2 000 mAU 500 mAU 50
1 500
1 000 25
500 250
0 0 0
0 2.5 5.0 7.5 0 2.5 5.0 7.5 0 1 2 3 4 5 6 7 8 9
t/min t/min t/min
9:木犀草素285.000 0>133.000 0(-)CE:35.0 9:木犀草素285.000 0>133.000 0(-)CE:35.0 9:木犀草素285.000 0>133.000 0(-)CE:35.0
25 000 2 500
400 C9
20 000 A9 2 000 B9
300
15 000
mAU 10 000 mAU 1 500 mAU 200
1 000
5 000 500 100
0 0 0
0 2.5 5.0 7.5 0 2.5 5.0 7.5 0 2.5 5.0 7.5
t/min t/min t/min
10:槲皮素301.000 0>150.900 0(-)CE:22.0 10:槲皮素301.000 0>150.900 0(-)CE:22.0 10:槲皮素301.000 0>150.900 0(-)CE:22.0
30 000 10 000
25 000 400 C10
A10 7 500 B10
20 000 300
mAU 15 000 mAU 5 000 mAU 200
10 000
2 500 100
5 000
0 0 0
0 2.5 5.0 7.5 0 2.5 5.0 7.5 0 2.5 5.0 7.5
t/min t/min t/min
11:芦丁609.000 0>301.000 0(-)CE:35.0 11:芦丁609.000 0>301.000 0(-)CE:35.0 11:芦丁609.000 0>301.000 0(-)CE:35.0
30 000
25 000 25
25 000 C11
20 000 A11 B11 20
20 000
mAU 15 000 mAU 15 000 mAU 15
10 000
10
10 000
5 000 5 000 5
0 0 0
0 2.5 5.0 7.5 0 2.5 5.0 7.5 0 1 2 3 4 5 6 7 8 9
t/min t/min t/min
A.混合对照品溶液 B.供试品溶液 C.空白溶液
续图1
·302 · China Pharmacy 2022 Vol. 33 No. 3 中国药房 2022年第33卷第3期